Synthesis and Catalysis for Alcohol Fuels

Synthesis and Catalysis for Alcohol Fuels

36 Pages · 2006 · 1.15 MB · English

SERVPR-233-2658 UC Category: 61f DE85012172 Synthesis and Catalysis for Alcohol Fuels 3. C. Smart August 1985 Prepared under Task No. 5150.20

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SERVPR-233-2658 UC Category: 61f DE85012172 Synthesis and Catalysis for Alcohol Fuels 3. C. Smart August 1985 Prepared under Task No. 5150.20 Solar Energy Research Institute A Division of Midwest Research Institute 161 7 Cole Boulevard Golden, Colorado 80401 Prepared for the U.S. Department of Energy Contract No. DE-AC02-83CH10093 PREFACE This progress report describes the chemical synthesis of new mate- rials and their evaluation as homogeneous and heterogeneous cata- lysts for the conversion of biomass-derived syngas (H2/CO) to alcohol fuels and fuel additives. This research was conducted by Alex Miedaner, Calvin Curtis, and James Smart of the Photocon- version Branch, Solar Fuels Division, SERT, and David Wickham and Scott Cowley of Colorado School of Mines. 1 n- J. u Smart, Leader Synthesis and Catalysis Task Approved for SOLAR ENERGY RESEARCH INSTITUTE Solar Fuels Research fiivisian Objective Active and selective catalysts are needed for the conversion of biomass- derived syngas (H2/CO) to alcohol fuels and fuel additives. The synthesis, characterization, and evaluation of selected dinuclear organometallic com- plexes of zirconium for reactions with H2/C0 have been completed in an effort to develop new homogeneous syngas catalysts. Discussion Screening studies and prelim.inary results have been obtained with hetero- geneous modified alumina-supported palladium catalysts for the production of higher alcohols from syngas. Following the recent discovery that selected early transition metal organometallic complexes with hydride ligands will stoichiometrically reduce carbon monoxide to coordinated ethylene glycolate, a two-carbon alcohol, we have demonstrated that dinuclear analogues of these

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